Determination Of Organic Structures By Physical Methods

Determination Of Organic Structures By Physical Methods

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Determination of Organic Structures by Physical Methods, Volume 6 is a six-chapter text that describes the refinements of some established physical methods for organic structure determination. The opening chapters examine the application of mass spectroscopy to amino acid sequencing of oligopeptides and the computerized organic structure retrieval. The following chapters discuss the historical developments, principles, instrumentation, and application of flash photolysis and 29Si nuclear magnetic resonance to structure determination. A chapter considers the relevant theory from which information on internuclear distances can be obtained and the steady-state measurements, transient methods, as well as the use of Fourier transform technique. This chapter also explores the application of nuclear overhauser effect measurements to structural and stereochemical problems. The concluding chapter deals with the liquid crystal structure determination using NMR spectroscopy. This work will be of value to organic and analytical chemists and researchers.This practice is in keeping with the tendencies and recommendations for NMR of other nuclei, 23 especially with the 8 ... Since in principle any of the common silicon compoundsa could be used as a reference standard, the choice should be anbsp;...

Title:Determination Of Organic Structures By Physical Methods
Author:F.C. Nachod
Publisher:Elsevier - 2012-12-02


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